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Synthesis and Characterization of a Soluble Vanadium-Containing Keggin Polyoxoniobate by ESI-MS and 51V NMR: (TMA)9[V3Nb12O42]center dot 18H2O
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2013 (English)In: European Journal of Inorganic Chemistry, ISSN 1434-1948, E-ISSN 1099-1948, no 10-11, SI, p. 1748-1753Article in journal (Refereed) Published
Abstract [en]

The vanadium-containing heteropolyoxoniobate (TMA)9[V3Nb12O42]center dot 18H2O was synthesised by hydrothermal reaction of V2O5 and hydrous niobium oxide in tetramethylammonium hydroxide solution. The cluster has an -Keggin structure with a central VO4 and two trans-bicapped VO5. The water-soluble product was characterised by X-ray crystallography, ESI-MS and both liquid- and solid-state 51V NMR spectroscopy. The solid- and solution-phase 51V NMR spectra indicate two major peaks corresponding to one VO4 and two VO5 sites.

Place, publisher, year, edition, pages
2013. no 10-11, SI, p. 1748-1753
Keywords [en]
Polyoxometalates; Niobium; Vanadium; Hydrothermal synthesis; NMR spectroscopy
National Category
Inorganic Chemistry
Identifiers
URN: urn:nbn:se:umu:diva-129120DOI: 10.1002/ejic.201201056OAI: oai:DiVA.org:umu-129120DiVA, id: diva2:1058642
Available from: 2016-12-21 Created: 2016-12-21 Last updated: 2018-06-09

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Ohlin, C. Andre

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