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Investigation of the titaniumdioxide-aqueous solution interface using XPS and cryogenics
Umeå University, Faculty of Science and Technology, Chemistry.
Umeå University, Faculty of Science and Technology, Chemistry.
2003 (English)In: Surface Science, Vol. 532-35, 1104-8 p.Article in journal (Refereed) Published
Abstract [en]

The sorption of Na[+] and Cl[-] electrolyte ions from an aqueous solution onto single crystal TiO[2] has been the subject of an investigation using XPS in combination with in situ cryogenics. In particular the samples were decontaminated from adventitious carbon by annealing at 600 °C prior to the exposure to aqueous solution. Further, the subsequent transfer of the sample to the spectrometer was performed in a liquid nitrogen filled hollow sample holder in order to preserve the chemistry and structure at the sample surface. The presence of an ionic layer consisting of H[2]O, Na[+] and Cl has been confirmed using angular dependent XPS, where the electrolyte ions are distributed in at least 2-3 monolayers.

Place, publisher, year, edition, pages
2003. Vol. 532-35, 1104-8 p.
Identifiers
URN: urn:nbn:se:umu:diva-9284OAI: oai:DiVA.org:umu-9284DiVA: diva2:148955
Available from: 2008-03-18 Created: 2008-03-18 Last updated: 2011-01-13Bibliographically approved

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