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Continuous hydrocyclization of aqueous levulinic acid to γ-valerolactone over bi-functional Ru/NbOPO4/SBA-15 catalyst under mild conditions
Umeå University, Faculty of Science and Technology, Department of Chemistry.
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2022 (English)In: Applied Catalysis A: General, ISSN 0926-860X, E-ISSN 1873-3875, Vol. 643, article id 118744Article in journal (Refereed) Published
Abstract [en]

Herein, we demonstrate that surface acid-base properties have marked effect upon the performance (activity, selectivity and stability) of supported Ru catalysts upon tandem hydrocyclization (hydrogenation-dehydration) of aqueous levulinic acid. A mesoporous bi-functional Ru/NbOPO4/SBA-15 catalyst incorporating highly dispersed Ru sites and well balanced strong Brønsted acidic sites (optimum B/L and M+S/W ratio) was identified, which outperformed the benchmark monofuncational (Ru/SBA-15, Ru/MCM-41) and physically blended bi-functional catalysts (Ru catalysts mixed with acid co-catalysts e.g. NbOPO4/Amberlyst-15). Further, the catalyst also demonstrated remarkable stability in a fixed-bed reactor, maintaining steady activity and γ-valerolactone selectivity (72-86%) during ca. 300 h time on stream (10 bar, 90-100 oC), corroborating its industrial potential. The exceptional performance and durability of the bi-functional catalyst was attributed to the presence of well dispersed hydrothermally and chemically stable acid (NbOPO4) and redox (Ru) sites.

Place, publisher, year, edition, pages
Elsevier, 2022. Vol. 643, article id 118744
Keywords [en]
Tandem hydrocyclization, γ-valerolactone, Supported Ru-catalysts, Bi-functional catalyst, Flow chemistry, Catalyst deactivation
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:umu:diva-197463DOI: 10.1016/j.apcata.2022.118744ISI: 000827290500001Scopus ID: 2-s2.0-85133252862OAI: oai:DiVA.org:umu-197463DiVA, id: diva2:1677950
Available from: 2022-06-28 Created: 2022-06-28 Last updated: 2023-09-05Bibliographically approved

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Samikannu, AjaikumarMikkola, Jyri-Pekka

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CiteExportLink to record
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