Characterization of Hydrogenated Fullerenes by NMR Spectroscopy
2010 (English)In: Fulleranes: The Hydrogenated Fullerenes / [ed] Franco Cataldo, Susana Iglesias-Groth, Dordrecht: Springer Netherlands, 2010, Vol. 2, 171-202 p.Chapter in book (Other academic)
NMR spectroscopy is so far the only analytical technique that has been used to get a detailed structural characterization of hydrogenated fullerenes. A substantial amount of information derived from different NMR experiments can thus be found in the literature for a number of fullerenes hydrogenated to various degrees. These studies have benefitted from the fact that chemical shifts of H-1 and C-13 and in some cases also He-3 can be used to obtain structural information of these compounds. Such results, together with discussions about different NMR experiments and general considerations regarding sample preparations, are summarized in this chapter. The unique information, both structural and physicochemical, that can be derived from different NMR experiments ensures that this technique will continue to be of central importance in characterization of hydrogenated fullerenes.
Place, publisher, year, edition, pages
Dordrecht: Springer Netherlands, 2010. Vol. 2, 171-202 p.
, Carbon Materials: Chemistry and Physics, ISSN 1875-0745 ; 2
Organic Chemistry Physical Chemistry
IdentifiersURN: urn:nbn:se:umu:diva-75732DOI: 10.1007/978-1-4020-9887-1_9ISI: 000277973900009ISBN: 978-1-4020-9886-4ISBN: 978-1-4020-9887-1OAI: oai:DiVA.org:umu-75732DiVA: diva2:635517