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Process for continuous hydrogenation of aqueous levulinic acid to gamma-valerolactone and its tandem conversion to high octane gasoline range hydrocarbons
Umeå University, Faculty of Science and Technology, Department of Chemistry.
Umeå University, Faculty of Science and Technology, Department of Chemistry.
Umeå University, Faculty of Science and Technology, Department of Chemistry.
Umeå University, Faculty of Science and Technology, Department of Chemistry.
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2024 (English)Patent (Other (popular science, discussion, etc.))
Abstract [en]

A Ru-loaded carbon material with characteristic surface chemistry (Br∅nsted acidic phosphate groups, Lewis basic N-groups selected from the group consisting of Lewis basic pyridinic, pyrrolic and quaternary N-groups and oxygen functional groups) is shown to exhibit excellent activity, selectivity and stability upon hydrogenation of aqueous levulinic acid (0.47M and 0.95M) to γ-alerolactone with near stochiometric H2 under mild conditions (80-95°C). The material demostrated remarkable stability in a fixed-bed reactor under continuous flow conditions, maintaining high activity, and γ-valerolactone selectivity during  ∼ 1250h time on stream operating at 3-5 bar, 80-95 °C and low H2/levulinic acid ratio (4-17). The exceptional catalytic performance and stability of the multifunctional Ru-catalyst was attributed to the unique surface chemistry of carbon support that stabilized the Ru nanoparticles on the surface nitrogen and oxygen defects, and promoted 4-hydroxypentanoic acid cyclization over acidic phosphate and RuOx/RuO2 sites.

Place, publisher, year, edition, pages
2024.
National Category
Chemical Sciences
Identifiers
URN: urn:nbn:se:umu:diva-228881OAI: oai:DiVA.org:umu-228881DiVA, id: diva2:1893101
Patent
WO 2024/160745 (2024-08-08)Available from: 2024-08-28 Created: 2024-08-28 Last updated: 2024-08-29Bibliographically approved

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Mikkola, Jyri-PekkaSamikannu, AjaikumarKonwar, Lakhya JyotiSiljebo, William

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