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High temperature exposure of MgO-based refractory material to biomass and coal ash with/without quicklime
Umeå universitet, Teknisk-naturvetenskapliga fakulteten, Institutionen för tillämpad fysik och elektronik. Centre for Sustainable Cement and Quicklime Production, Umeå university, Sweden; Thermochemical Energy Conversion Laboratory, Umeå University, Sweden; Department of Materials Science and Engineering, School of Industrial Engineering and Management, KTH Royal Institute of Technology, Stockholm, Sweden.ORCID-id: 0000-0002-3342-6257
Umeå universitet, Teknisk-naturvetenskapliga fakulteten, Institutionen för tillämpad fysik och elektronik. Centre for Sustainable Cement and Quicklime Production, Umeå university, Sweden; Thermochemical Energy Conversion Laboratory, Umeå University, Sweden.ORCID-id: 0000-0003-1170-2203
Umeå universitet, Teknisk-naturvetenskapliga fakulteten, Institutionen för tillämpad fysik och elektronik. Centre for Sustainable Cement and Quicklime Production, Umeå university, Sweden; Thermochemical Energy Conversion Laboratory, Umeå University, Sweden; Swedish Mineral Processing Research Association - MinFo, BOX 47055, Stockholm, Sweden.ORCID-id: 0000-0002-8230-8847
Umeå universitet, Teknisk-naturvetenskapliga fakulteten, Institutionen för tillämpad fysik och elektronik. Centre for Sustainable Cement and Quicklime Production, Umeå university, Sweden; Thermochemical Energy Conversion Laboratory, Umeå University, Sweden.ORCID-id: 0000-0002-0555-5924
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2024 (Engelska)Ingår i: Ceramics International, ISSN 0272-8842, E-ISSN 1873-3956Artikel i tidskrift (Refereegranskat) Epub ahead of print
Abstract [en]

Refractory liner bricks in the hot zone of rotary lime kilns can sustain wear and corrosion during contact with fuel ashes and quicklime (QL), a product composed mainly of CaO. The effects on a MgO-based refractory after exposure at 1400 °C for 96 h to olive pomace ash (OPA) and coal ash (CA), with and without QL, were investigated. Exposure of the refractory to only OPA caused slag intrusion with no ash deposits remaining on top, while CaMgSiO4 (monticellite) was also identified as a new phase. When exposed to only CA, the refractory exhibited dissolution into the molten slag and 0.5–2 mm cracks were found on the surface interfacing the ash. Mg2SiO4 (forsterite) and CaMgSiO4 were identified as new formed phases. Exposure of the refractory to OPA + QL and CA + QL caused less slag intrusion and substantial amounts of ash/QL deposit remained afterwards. No new phases were identified. The differences in interactions between the exposure materials and refractory were supported by thermochemical equilibrium analysis. Apparent Ca-Si–rich or Ca-rich melts were found in all the exposed samples, but potassium (K) was found to be depleted in all samples, including those involving OPA, which was rich in K. Furthermore, with the exception of exposure to only CA, the other exposures caused the cold crushing strength (CCS) of the refractory to increase compared to its original value. This was attributed to the sintering of the refractory microstructure. The CCS of the refractory decreased after exposure to only CA. The findings of this study enhance understanding of how CA and OPA impact MgO refractories in lime kilns, supporting initiatives aiming at reducing fossil fuel use. The results are encouraging and motivate further investigation.

Ort, förlag, år, upplaga, sidor
Elsevier, 2024.
Nyckelord [en]
Crushing strength, Fuel ashes, Lime kilns, MgO refractory, Refractory corrosion
Nationell ämneskategori
Metallurgi och metalliska material
Identifikatorer
URN: urn:nbn:se:umu:diva-232780DOI: 10.1016/j.ceramint.2024.11.342Scopus ID: 2-s2.0-85210741543OAI: oai:DiVA.org:umu-232780DiVA, id: diva2:1922167
Forskningsfinansiär
Bio4EnergyEnergimyndighetenTillgänglig från: 2024-12-18 Skapad: 2024-12-18 Senast uppdaterad: 2025-01-12

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Kumar Wagri, NareshCarlborg, MarkusEriksson, MatiasMa, CharlieBroström, MarkusAndersson, Britt M.

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Kumar Wagri, NareshCarlborg, MarkusEriksson, MatiasMa, CharlieBroström, MarkusAndersson, Britt M.
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